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Solid-state NMR studies of supercapacitors.

Solid state nuclear magnetic resonance

Griffin JM, Forse AC, Grey CP.
PMID: 26974032
Solid State Nucl Magn Reson. 2016 Apr-May;74:16-35. doi: 10.1016/j.ssnmr.2016.03.003. Epub 2016 Mar 04.

Electrochemical double-layer capacitors, or 'supercapacitors' are attracting increasing attention as high-power energy storage devices for a wide range of technological applications. These devices store charge through electrostatic interactions between liquid electrolyte ions and the surfaces of porous carbon electrodes....

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Griffin JM, Forse AC, Grey CP. Solid-state NMR studies of supercapacitors. Solid State Nucl Magn Reson. 2016;74:16-35doi: 10.1016/j.ssnmr.2016.03.003.
Griffin, J. M., Forse, A. C., & Grey, C. P. (2016). Solid-state NMR studies of supercapacitors. Solid state nuclear magnetic resonance, 7416-35. https://doi.org/10.1016/j.ssnmr.2016.03.003
Griffin, John M, et al. "Solid-state NMR studies of supercapacitors." Solid state nuclear magnetic resonance vol. 74 (2016): 16-35. doi: https://doi.org/10.1016/j.ssnmr.2016.03.003
Griffin JM, Forse AC, Grey CP. Solid-state NMR studies of supercapacitors. Solid State Nucl Magn Reson. 2016 Apr-May;74:16-35. doi: 10.1016/j.ssnmr.2016.03.003. Epub 2016 Mar 04. PMID: 26974032.
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Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state (31)P NMR.

Solid state nuclear magnetic resonance

Tassi M, Reekmans G, Carleer R, Adriaensens P.
PMID: 27497944
Solid State Nucl Magn Reson. 2016 Sep;78:50-55. doi: 10.1016/j.ssnmr.2016.07.001. Epub 2016 Jul 12.

For the first time, an absolute quantification of hybrid materials obtained from the reaction of phenylphosphonic acid (PPA) with TiO2 nanoparticles under different reaction conditions is reported. Next to the amount of PPA involved in grafting to the TiO2...

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Tassi M, Reekmans G, Carleer R, et al. Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state (31)P NMR. Solid State Nucl Magn Reson. 2016;78:50-55doi: 10.1016/j.ssnmr.2016.07.001.
Tassi, M., Reekmans, G., Carleer, R., & Adriaensens, P. (2016). Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state (31)P NMR. Solid state nuclear magnetic resonance, 7850-55. https://doi.org/10.1016/j.ssnmr.2016.07.001
Tassi, Marco, et al. "Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state (31)P NMR." Solid state nuclear magnetic resonance vol. 78 (2016): 50-55. doi: https://doi.org/10.1016/j.ssnmr.2016.07.001
Tassi M, Reekmans G, Carleer R, Adriaensens P. Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state (31)P NMR. Solid State Nucl Magn Reson. 2016 Sep;78:50-55. doi: 10.1016/j.ssnmr.2016.07.001. Epub 2016 Jul 12. PMID: 27497944.
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Probing intermolecular interactions in a diethylcarbamazine citrate salt by fast MAS .

Solid state nuclear magnetic resonance

Venâncio T, Oliveira LM, Ellena J, Boechat N, Brown SP.
PMID: 28342733
Solid State Nucl Magn Reson. 2017 Oct;87:73-79. doi: 10.1016/j.ssnmr.2017.02.006. Epub 2017 Mar 02.

Fast magic-angle spinning (MAS) NMR is used to probe intermolecular interactions in a diethylcarbamazine salt, that is widely used as a treatment against adult worms of Wuchereria bancrofti which cause a common disease in tropical countries named filariasis. Specifically,...

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Venâncio T, Oliveira LM, Ellena J, et al. Probing intermolecular interactions in a diethylcarbamazine citrate salt by fast MAS . Solid State Nucl Magn Reson. 2017;87:73-79doi: 10.1016/j.ssnmr.2017.02.006.
Venâncio, T., Oliveira, L. M., Ellena, J., Boechat, N., & Brown, S. P. (2017). Probing intermolecular interactions in a diethylcarbamazine citrate salt by fast MAS . Solid state nuclear magnetic resonance, 8773-79. https://doi.org/10.1016/j.ssnmr.2017.02.006
Venâncio, Tiago, et al. "Probing intermolecular interactions in a diethylcarbamazine citrate salt by fast MAS ." Solid state nuclear magnetic resonance vol. 87 (2017): 73-79. doi: https://doi.org/10.1016/j.ssnmr.2017.02.006
Venâncio T, Oliveira LM, Ellena J, Boechat N, Brown SP. Probing intermolecular interactions in a diethylcarbamazine citrate salt by fast MAS . Solid State Nucl Magn Reson. 2017 Oct;87:73-79. doi: 10.1016/j.ssnmr.2017.02.006. Epub 2017 Mar 02. PMID: 28342733.
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γ-Independent through-space hetero-nuclear correlation between spin-1/2 and quadrupolar nuclei in solids.

Solid state nuclear magnetic resonance

Nagashima H, Lilly Thankamony AS, Trébosc J, Pourpoint F, Lafon O, Amoureux JP.
PMID: 28666574
Solid State Nucl Magn Reson. 2017 Jul - Aug;84:216-226. doi: 10.1016/j.ssnmr.2017.06.002. Epub 2017 Jun 19.

We introduce novel sequences using indirect detection to correlate quadrupolar nuclei and spin-1/2 isotopes, other than

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Nagashima H, Lilly Thankamony AS, Trébosc J, et al. γ-Independent through-space hetero-nuclear correlation between spin-1/2 and quadrupolar nuclei in solids. Solid State Nucl Magn Reson. 2017;84:216-226doi: 10.1016/j.ssnmr.2017.06.002.
Nagashima, H., Lilly Thankamony, A. S., Trébosc, J., Pourpoint, F., Lafon, O., & Amoureux, J. P. (2017). γ-Independent through-space hetero-nuclear correlation between spin-1/2 and quadrupolar nuclei in solids. Solid state nuclear magnetic resonance, 84216-226. https://doi.org/10.1016/j.ssnmr.2017.06.002
Nagashima, Hiroki, et al. "γ-Independent through-space hetero-nuclear correlation between spin-1/2 and quadrupolar nuclei in solids." Solid state nuclear magnetic resonance vol. 84 (2017): 216-226. doi: https://doi.org/10.1016/j.ssnmr.2017.06.002
Nagashima H, Lilly Thankamony AS, Trébosc J, Pourpoint F, Lafon O, Amoureux JP. γ-Independent through-space hetero-nuclear correlation between spin-1/2 and quadrupolar nuclei in solids. Solid State Nucl Magn Reson. 2017 Jul - Aug;84:216-226. doi: 10.1016/j.ssnmr.2017.06.002. Epub 2017 Jun 19. PMID: 28666574.
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Quadrupolar solid-state NMR and repetitive experiments: Some aspects in the Liouville space. Application to spins I=1.

Solid state nuclear magnetic resonance

Odin C.
PMID: 28081936
Solid State Nucl Magn Reson. 2017 Jul - Aug;84:73-82. doi: 10.1016/j.ssnmr.2016.12.012. Epub 2016 Dec 29.

The aim of this work is to generalize the Ernst-Anderson model developed to account of the steady-state regime of isolated spins I=1/2 subject to a train of strictly identical pulse sequences separated by free evolution periods of same duration....

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Odin C. Quadrupolar solid-state NMR and repetitive experiments: Some aspects in the Liouville space. Application to spins I=1. Solid State Nucl Magn Reson. 2016;84:73-82doi: 10.1016/j.ssnmr.2016.12.012.
Odin, C. (2017). Quadrupolar solid-state NMR and repetitive experiments: Some aspects in the Liouville space. Application to spins I=1. Solid state nuclear magnetic resonance, 8473-82. https://doi.org/10.1016/j.ssnmr.2016.12.012
Odin, Christophe. "Quadrupolar solid-state NMR and repetitive experiments: Some aspects in the Liouville space. Application to spins I=1." Solid state nuclear magnetic resonance vol. 84 (2017): 73-82. doi: https://doi.org/10.1016/j.ssnmr.2016.12.012
Odin C. Quadrupolar solid-state NMR and repetitive experiments: Some aspects in the Liouville space. Application to spins I=1. Solid State Nucl Magn Reson. 2017 Jul - Aug;84:73-82. doi: 10.1016/j.ssnmr.2016.12.012. Epub 2016 Dec 29. PMID: 28081936.
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Simulating spin dynamics in organic solids under heteronuclear decoupling.

Solid state nuclear magnetic resonance

Frantsuzov I, Ernst M, Brown SP, Hodgkinson P.
PMID: 26073419
Solid State Nucl Magn Reson. 2015 Sep;70:28-37. doi: 10.1016/j.ssnmr.2015.05.003. Epub 2015 May 15.

Although considerable progress has been made in simulating the dynamics of multiple coupled nuclear spins, predicting the evolution of nuclear magnetisation in the presence of radio-frequency decoupling remains challenging. We use exact numerical simulations of the spin dynamics under...

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Frantsuzov I, Ernst M, Brown SP, et al. Simulating spin dynamics in organic solids under heteronuclear decoupling. Solid State Nucl Magn Reson. 2015;70:28-37doi: 10.1016/j.ssnmr.2015.05.003.
Frantsuzov, I., Ernst, M., Brown, S. P., & Hodgkinson, P. (2015). Simulating spin dynamics in organic solids under heteronuclear decoupling. Solid state nuclear magnetic resonance, 7028-37. https://doi.org/10.1016/j.ssnmr.2015.05.003
Frantsuzov, Ilya, et al. "Simulating spin dynamics in organic solids under heteronuclear decoupling." Solid state nuclear magnetic resonance vol. 70 (2015): 28-37. doi: https://doi.org/10.1016/j.ssnmr.2015.05.003
Frantsuzov I, Ernst M, Brown SP, Hodgkinson P. Simulating spin dynamics in organic solids under heteronuclear decoupling. Solid State Nucl Magn Reson. 2015 Sep;70:28-37. doi: 10.1016/j.ssnmr.2015.05.003. Epub 2015 May 15. PMID: 26073419.
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Nuclear polarization by optical pumping in InP:Fe above liquid nitrogen temperature.

Solid state nuclear magnetic resonance

Yoon D, Soundararajan M, Ansermet JP.
PMID: 26113254
Solid State Nucl Magn Reson. 2015 Sep;70:48-52. doi: 10.1016/j.ssnmr.2015.06.003. Epub 2015 Jun 09.

Hyperpolarized nuclear spins are observed in optically pumped iron-doped InP from 70K to 140K. (31)P NMR was carried out at 9.28T (159.8MHz) during optical excitation with circularly polarized light, using a laser diode (λ∼830nm) as a source. The enhancement...

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Yoon D, Soundararajan M, Ansermet JP. Nuclear polarization by optical pumping in InP:Fe above liquid nitrogen temperature. Solid State Nucl Magn Reson. 2015;70:48-52doi: 10.1016/j.ssnmr.2015.06.003.
Yoon, D., Soundararajan, M., & Ansermet, J. P. (2015). Nuclear polarization by optical pumping in InP:Fe above liquid nitrogen temperature. Solid state nuclear magnetic resonance, 7048-52. https://doi.org/10.1016/j.ssnmr.2015.06.003
Yoon, Dongyoung, et al. "Nuclear polarization by optical pumping in InP:Fe above liquid nitrogen temperature." Solid state nuclear magnetic resonance vol. 70 (2015): 48-52. doi: https://doi.org/10.1016/j.ssnmr.2015.06.003
Yoon D, Soundararajan M, Ansermet JP. Nuclear polarization by optical pumping in InP:Fe above liquid nitrogen temperature. Solid State Nucl Magn Reson. 2015 Sep;70:48-52. doi: 10.1016/j.ssnmr.2015.06.003. Epub 2015 Jun 09. PMID: 26113254.
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Dynamics of [C3H5N2]6[Bi4Br18] by means of (1)H NMR relaxometry and quadrupole relaxation enhancement.

The Journal of chemical physics

Masierak W, Florek-Wojciechowska M, Oglodek I, Jakubas R, Privalov AF, Kresse B, Fujara F, Kruk D.
PMID: 26026454
J Chem Phys. 2015 May 28;142(20):204503. doi: 10.1063/1.4919966.

(1)H spin-lattice field cycling relaxation dispersion experiments in the intermediate phase II of the solid [C3H5N2]6[Bi4Br18] are presented. Two motional processes have been identified from the (1)H spin-lattice relaxation dispersion profiles and quantitatively described. It has been concluded that...

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Masierak W, Florek-Wojciechowska M, Oglodek I, et al. Dynamics of [C3H5N2]6[Bi4Br18] by means of (1)H NMR relaxometry and quadrupole relaxation enhancement. J Chem Phys. 2015;142(20):204503doi: 10.1063/1.4919966.
Masierak, W., Florek-Wojciechowska, M., Oglodek, I., Jakubas, R., Privalov, A. F., Kresse, B., Fujara, F., & Kruk, D. (2015). Dynamics of [C3H5N2]6[Bi4Br18] by means of (1)H NMR relaxometry and quadrupole relaxation enhancement. The Journal of chemical physics, 142(20), 204503. https://doi.org/10.1063/1.4919966
Masierak, W, et al. "Dynamics of [C3H5N2]6[Bi4Br18] by means of (1)H NMR relaxometry and quadrupole relaxation enhancement." The Journal of chemical physics vol. 142,20 (2015): 204503. doi: https://doi.org/10.1063/1.4919966
Masierak W, Florek-Wojciechowska M, Oglodek I, Jakubas R, Privalov AF, Kresse B, Fujara F, Kruk D. Dynamics of [C3H5N2]6[Bi4Br18] by means of (1)H NMR relaxometry and quadrupole relaxation enhancement. J Chem Phys. 2015 May 28;142(20):204503. doi: 10.1063/1.4919966. PMID: 26026454.
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Solid-state NMR strategies for the structural characterization of paramagnetic NO adducts of Frustrated Lewis Pairs (FLPs).

Solid state nuclear magnetic resonance

Wiegand T, Sajid M, Kehr G, Erker G, Eckert H.
PMID: 24815176
Solid State Nucl Magn Reson. 2014 Jul-Sep;61:19-27. doi: 10.1016/j.ssnmr.2014.04.001. Epub 2014 Apr 19.

By N,N addition of NO to the norbonane annulated borane-phosphane Frustrated Lewis pair (FLP) 1 a five-membered heterocyclic persistent aminoxyl radical 2 and its diamagnetic hydroxylamine reduction product 3 are prepared, and the comprehensive multinuclear solid state NMR characterization...

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Wiegand T, Sajid M, Kehr G, et al. Solid-state NMR strategies for the structural characterization of paramagnetic NO adducts of Frustrated Lewis Pairs (FLPs). Solid State Nucl Magn Reson. 2014;61:19-27doi: 10.1016/j.ssnmr.2014.04.001.
Wiegand, T., Sajid, M., Kehr, G., Erker, G., & Eckert, H. (2014). Solid-state NMR strategies for the structural characterization of paramagnetic NO adducts of Frustrated Lewis Pairs (FLPs). Solid state nuclear magnetic resonance, 6119-27. https://doi.org/10.1016/j.ssnmr.2014.04.001
Wiegand, Thomas, et al. "Solid-state NMR strategies for the structural characterization of paramagnetic NO adducts of Frustrated Lewis Pairs (FLPs)." Solid state nuclear magnetic resonance vol. 61 (2014): 19-27. doi: https://doi.org/10.1016/j.ssnmr.2014.04.001
Wiegand T, Sajid M, Kehr G, Erker G, Eckert H. Solid-state NMR strategies for the structural characterization of paramagnetic NO adducts of Frustrated Lewis Pairs (FLPs). Solid State Nucl Magn Reson. 2014 Jul-Sep;61:19-27. doi: 10.1016/j.ssnmr.2014.04.001. Epub 2014 Apr 19. PMID: 24815176.
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On the role of experimental imperfections in constructing (1)H spin diffusion NMR plots for domain size measurements.

Solid state nuclear magnetic resonance

Nieuwendaal RC.
PMID: 27039203
Solid State Nucl Magn Reson. 2016 Jun-Jul;76:29-36. doi: 10.1016/j.ssnmr.2016.03.006. Epub 2016 Mar 24.

We discuss the precision of 1D chemical-shift-based (1)H spin diffusion NMR experiments as well as straightforward experimental protocols for reducing errors. The (1)H spin diffusion NMR experiments described herein are useful for samples that contain components with significant spectral...

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Nieuwendaal RC. On the role of experimental imperfections in constructing (1)H spin diffusion NMR plots for domain size measurements. Solid State Nucl Magn Reson. 2016;76:29-36doi: 10.1016/j.ssnmr.2016.03.006.
Nieuwendaal, R. C. (2016). On the role of experimental imperfections in constructing (1)H spin diffusion NMR plots for domain size measurements. Solid state nuclear magnetic resonance, 7629-36. https://doi.org/10.1016/j.ssnmr.2016.03.006
Nieuwendaal, Ryan C. "On the role of experimental imperfections in constructing (1)H spin diffusion NMR plots for domain size measurements." Solid state nuclear magnetic resonance vol. 76 (2016): 29-36. doi: https://doi.org/10.1016/j.ssnmr.2016.03.006
Nieuwendaal RC. On the role of experimental imperfections in constructing (1)H spin diffusion NMR plots for domain size measurements. Solid State Nucl Magn Reson. 2016 Jun-Jul;76:29-36. doi: 10.1016/j.ssnmr.2016.03.006. Epub 2016 Mar 24. PMID: 27039203; PMCID: PMC4903914.
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Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS.

Solid state nuclear magnetic resonance

Pandey MK, Yarava JR, Zhang R, Ramamoorthy A, Nishiyama Y.
PMID: 27017575
Solid State Nucl Magn Reson. 2016 Jun-Jul;76:1-6. doi: 10.1016/j.ssnmr.2016.03.001. Epub 2016 Mar 16.

Chemical shift anisotropy (CSA) tensors offer a wealth of information for structural and dynamics studies of a variety of chemical and biological systems. In particular, CSA of amide protons can provide piercing insights into hydrogen-bonding interactions that vary with...

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Pandey MK, Yarava JR, Zhang R, et al. Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS. Solid State Nucl Magn Reson. 2016;76:1-6doi: 10.1016/j.ssnmr.2016.03.001.
Pandey, M. K., Yarava, J. R., Zhang, R., Ramamoorthy, A., & Nishiyama, Y. (2016). Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS. Solid state nuclear magnetic resonance, 761-6. https://doi.org/10.1016/j.ssnmr.2016.03.001
Pandey, Manoj Kumar, et al. "Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS." Solid state nuclear magnetic resonance vol. 76 (2016): 1-6. doi: https://doi.org/10.1016/j.ssnmr.2016.03.001
Pandey MK, Yarava JR, Zhang R, Ramamoorthy A, Nishiyama Y. Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS. Solid State Nucl Magn Reson. 2016 Jun-Jul;76:1-6. doi: 10.1016/j.ssnmr.2016.03.001. Epub 2016 Mar 16. PMID: 27017575; PMCID: PMC4903906.
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Adding a lens Improves spinning speed characterization.

Solid state nuclear magnetic resonance

Mihaliuk E, Gullion T.
PMID: 26382300
Solid State Nucl Magn Reson. 2015 Nov;72:4-8. doi: 10.1016/j.ssnmr.2015.09.004. Epub 2015 Sep 08.

Highly stable sample rotation is important in many solid-state NMR experiments. Whether the necessary stability is achieved is not always clear. Typically only an average frequency over some time interval (often relatively long and unknown) is available from the...

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Mihaliuk E, Gullion T. Adding a lens Improves spinning speed characterization. Solid State Nucl Magn Reson. 2015;72:4-8doi: 10.1016/j.ssnmr.2015.09.004.
Mihaliuk, E., & Gullion, T. (2015). Adding a lens Improves spinning speed characterization. Solid state nuclear magnetic resonance, 724-8. https://doi.org/10.1016/j.ssnmr.2015.09.004
Mihaliuk, Eugene, and Gullion, Terry. "Adding a lens Improves spinning speed characterization." Solid state nuclear magnetic resonance vol. 72 (2015): 4-8. doi: https://doi.org/10.1016/j.ssnmr.2015.09.004
Mihaliuk E, Gullion T. Adding a lens Improves spinning speed characterization. Solid State Nucl Magn Reson. 2015 Nov;72:4-8. doi: 10.1016/j.ssnmr.2015.09.004. Epub 2015 Sep 08. PMID: 26382300.
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